Benzene, 1,4-bis(phenylthio)- synthesis
15synthesis methods
- Product Name:Benzene, 1,4-bis(phenylthio)-
- CAS Number:3459-94-7
- Molecular formula:C18H14S2
- Molecular Weight:294.43
Yield:3459-94-7 99%
Reaction Conditions:
with 1,2,3,4-tetrahydroquinolin-8-ol;caesium carbonate;copper(I) bromide in N,N-dimethyl-formamide at 130; for 48 h;Inert atmosphere;chemoselective reaction;
References:
Li, Yaming;Li, Xiaoying;Wang, Huifeng;Chen, Tao;Xie, Yusheng [Synthesis,2010,# 21,art. no. F10410SS,p. 3602 - 3608] Location in patent:supporting information; experimental part
