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ChemicalBook CAS DataBase List Benzeneruthenium(II) chloride dimer

Benzeneruthenium(II) chloride dimer synthesis

2synthesis methods
-

Yield:37366-09-9 81%

Reaction Conditions:

in ethanoltreating soln. of RuCl3 (0.0065 mol) in 90% alc. with 1.3-cyclohexadiene (0.0065 mol), stirring mixt. for 3 h at 45°C; pptn., filtering after 12 h, washing with alc. and ether, drying in vac.; elem. anal.;

References:

Bezrukova, A. A.;Khandkarova, V. S.;Andrianov, V. G.;Struchkov, Yu. T.;Rubezhov, A. Z. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1987,vol. 36,p. 1922 - 1926][Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.),1987,p. 2071 - 2076]

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