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ChemicalBook CAS DataBase List Benzoic acid, 2-chloro-4-fluoro-, ethyl ester
167758-87-4

Benzoic acid, 2-chloro-4-fluoro-, ethyl ester synthesis

3synthesis methods
-

Yield:167758-87-4 61%

Reaction Conditions:

with N-chloro-succinimide;trifluorormethanesulfonic acid;palladium diacetate;N-fluoropyridinium triflate in 1,2-dichloro-ethane at 90; for 6 h;Sealed tube;regioselective reaction;

References:

Sun, Xiuyun;Shan, Gang;Sun, Yonghui;Rao, Yu [Angewandte Chemie - International Edition,2013,vol. 52,# 16,p. 4440 - 4444][Angew. Chem.,2013,vol. 125,# 16,p. 4536 - 4540,5] Location in patent:supporting information

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