ChemicalBook CAS DataBase List BICYCLO[2.2.2]OCTANE

BICYCLO[2.2.2]OCTANE synthesis

13synthesis methods

Product Name:BICYCLO[2.2.2]OCTANE
CAS Number:280-33-1
Molecular formula:C8H14
Molecular Weight:110.2

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Yield:-

Steps:

S.9 SYNTHESIS EXAMPLE 9
SYNTHESIS EXAMPLE 9 A ketone compound was prepared in the same manner as in Synthesis Example 8, except that 50 g of diethyl ketone was used in place of methyl ethyl ketone. The ketone substance was reduced to obtain 6.4 g of a colorless liquid having a boiling point of 115° C. to 125° C. at 1 mmHg. The colorless liquid was a mixture of 1-substituted-2-methyl-3-hydroxy-1-pentenes containing a bicyclo[2,2,2]octane substituent which were the same as those obtained in Synthesis Example 8. The colorless liquid had a camphor-like and sandalwood-like odor, and the instrumental analytical values thereof were as follows: MS: M⁺ =264 m/e. IR: 3320 cm^-1.

References:

Takasago Perfumery Co., Ltd. US4434306, 1984, A