Bis(2-methylaminophenyl)amine synthesis
2synthesis methods
- Product Name:Bis(2-methylaminophenyl)amine
- CAS Number:1296883-59-4
- Molecular formula:C14H17N3
- Molecular Weight:227.3
Yield:1296883-59-4 92%
Reaction Conditions:
Stage #1: formaldehyd;bis(2-aminophenyl)aminewith sodium methylate in methanol at 0; for 1 h;Reflux;
Stage #2: with sodium tetrahydroborate in methanol at 0; for 1 h;Reflux;
References:
Zhao, Wei;McCarthy, Sean M.;Lai, Ting Yi;Yennawar, Hemant P.;Radosevich, Alexander T. [Journal of the American Chemical Society,2014,vol. 136,# 50,p. 17634 - 17644] Location in patent:supporting information
