Boc-Phe-Phe-OH synthesis
- Product Name:Boc-Phe-Phe-OH
- CAS Number:13122-90-2
- Molecular formula:C23H28N2O5
- Molecular Weight:412.48
13122-89-9
13122-90-2
General procedure for the synthesis of Boc-L-phenylalanyl-phenylalanine from methyl (tert-butoxycarbonyl)phenylpropionyl-phenylpropionate: to a solution of methanol (20 ml) containing methyl 2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropionamido)-3-phenylpropionate (2.0 g, 4.69 mmol), sodium hydroxide (0.38 g, 9.38 mmol) in water (10 ml) solution and the reaction temperature was maintained at 25-30°C. The reaction mixture was stirred at the same temperature for 1 hour. After completion of the reaction, methanol was removed by evaporation and the remaining aqueous layer was acidified with citric acid solution until the solid precipitated. The solid product was collected by filtration and dried to give Boc-L-phenylalanyl-phenylalanine as a white solid (1.89 g, 98% yield); ESI-MS: 413.2 (M + H).
13122-89-9
13 suppliers
inquiry
13122-90-2
124 suppliers
$26.00/250mg
24424-99-5
867 suppliers
$13.50/25G
2577-40-4
173 suppliers
$5.00/25mg
13122-90-2
124 suppliers
$26.00/250mg
63-91-2
926 suppliers
$10.00/100G
3674-06-4
108 suppliers
$19.00/5g
13122-90-2
124 suppliers
$26.00/250mg
13734-34-4
555 suppliers
$5.50/5g
13122-90-2
124 suppliers
$26.00/250mg