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ChemicalBook CAS DataBase List BRN 1750035
2594-20-9

BRN 1750035 synthesis

3synthesis methods
-

Yield:2594-20-9 73%

Reaction Conditions:

Stage #1: 3-amino-4-pyridinylcarbamic acid ethyl esterwith nitrosonium tetrafluoroborate in acetonitrile at 0; for 0.333333 h;
Stage #2: isopropylamine in acetonitrile at 20;

References:

Holt, Jarle;Fiksdahl, Anne [Journal of Heterocyclic Chemistry,2006,vol. 43,# 2,p. 417 - 423]