CHLOROBENZENE-4-D1 synthesis
- Product Name:CHLOROBENZENE-4-D1
- CAS Number:13122-34-4
- Molecular formula:C6H4ClD
- Molecular Weight:113.56
106-39-8
462 suppliers
$14.00/5g
13122-34-4
16 suppliers
$76.00/25mg
Yield:13122-34-4 88%
Reaction Conditions:
with neopentyl chloride;sodium in hexane;paraffin oil at 0; for 0.5 h;
Steps:
6.5 Experiment Number 5
0.25 mmol (1.0 molar equivalent) of 1-bromo-4-chlorobenzene was added to neopentyl sodium synthesized in the same manner as in Experiment Number 1, and the mixture was reacted in hexane at 0° C. for 30 minutes to synthesize 4-chlorophenyl sodium. A product was evaluated by trapping the product with 0.3 mmol (1.2 molar equivalents) of chlorodimethylphenylsilane, performing 1H NMR measurement and calculating a yield, in the same manner as in Examination Example 2. The results are shown in FIG. 7. As shown in FIG. 7, the yield of 4-chlorophenyl sodium was 88%.
References:
US2021/388004,2021,A1 Location in patent:Paragraph 0027; 0101; 0106
56075-36-6
0 suppliers
inquiry
13122-34-4
16 suppliers
$76.00/25mg
873-77-8
151 suppliers
$65.29/100ml
13122-34-4
16 suppliers
$76.00/25mg
637-87-6
302 suppliers
$38.00/10g
13122-34-4
16 suppliers
$76.00/25mg
1679-18-1
617 suppliers
$10.00/1g
13122-34-4
16 suppliers
$76.00/25mg