CHLOROTITANIUM TRIISOPROPOXIDE synthesis
- Product Name:CHLOROTITANIUM TRIISOPROPOXIDE
- CAS Number:20717-86-6
- Molecular formula:C9H21ClO3Ti
- Molecular Weight:260.58
546-68-9
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20717-86-6
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Yield:-
Steps:
7 Example 7
Example 7 At 25-40° C. and under an atmosphere of nitrogen, titanium tetrachloride (0.77 ml) was added with stirring (careful, exothermic reaction) over a period of 5 minutes to titanium tetraisopropoxide (6.23 ml), and the mixture was briefly (for 5 minutes) heated with stirring to 80° C. The chlorotriisopropoxytitanium, which was formed quantitatively, was cooled to room temperature, and at room temperature, a solution of N-benzyl-3-pyrroline (5.2 g) and dibenzylformamide (7.3 g) in anhydrous tetrahydrofuran (80 ml) was added to it over a period of 5 minutes, and a solution of cyclohexylmagnesium bromide in ether (39.2 ml, 2.1 M) was then added at 30-40° C. over a period of 30 minutes (exothermic reaction).
References:
Bayer Aktiengesellschaft US6043393, 2000, A
546-68-9
336 suppliers
$12.00/5g
7550-45-0
302 suppliers
$10.00/10g
20717-86-6
108 suppliers
$62.00/25g