ChemicalBook CAS DataBase List Dibenzyl azodicarboxylate

Dibenzyl azodicarboxylate synthesis

2synthesis methods

Product Name:Dibenzyl azodicarboxylate
CAS Number:2449-05-0
Molecular formula:C16H14N2O4
Molecular Weight:298.29

PIDA (phenyliodine diacetate) and DCM (dichloromethane) were added to compound dibenzyl hydrazine-1,2-dicarboxylate, and the mixture was reacted with stirring at room temperature for 30 minutes to obtain DBAD (dibenzyl azodicarboxylate) in a yield of 97%.

5394-50-3
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2449-05-0
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$5.00/1g

Yield:2449-05-0 97%

Reaction Conditions:

with [bis(acetoxy)iodo]benzene in dichloromethane at 20; for 0.5 h;

Steps:

1 [Experimental Example 1]

PIDA (phenyliodine diacetate) and DCM (dichloromethane) were added to Compound 5, and the mixture was reacted with stirring at room temperature for 30 minutes to obtain DBAD (dibenzyl azodicarboxylate) in a yield of 97%.

References:

KR2021/153284,2021,A Location in patent:Paragraph 0269-0270; 0273-0274

501-53-1
394 suppliers
$10.00/1g

2449-05-0
228 suppliers
$5.00/1g

References

Dibenzyl azodicarboxylate Related Search:

Benzylparaben Diethyl azodicarboxylate Benzyl benzoate Carbobenzoxyhydrazide Palladium (II) Acetate Benzophenone Sodium acetate trihydrate Di-tert-Butyl azodicarboxylate 1,1'-(Azodicarbonyl)-dipiperidine Diisopropyl azodicarboxylate