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DIMETHYL THIOPHOSPHONATE 97 synthesis

4synthesis methods
-

Yield:5930-72-3 69%

Reaction Conditions:

with Lawessons reagent in benzene; for 0.75 h;Heating;or 30 d, r.t.;

References:

Zabirov, N. G.;Cherkasov, R. A.;Khalikov, I. S.;Pudovik, A. N. [Journal of general chemistry of the USSR,1989,vol. 59,p. 1327 - 1332][Zhurnal Obshchei Khimii,1989,vol. 59,# 7,p. 1493 - 1500]