ChemicalBook CAS DataBase List Dimethylamine hydrochloride

Dimethylamine hydrochloride synthesis

6synthesis methods

Product Name:Dimethylamine hydrochloride
CAS Number:506-59-2
Molecular formula:C2H8ClN
Molecular Weight:81.54

Dimethylamine hydrochloride is obtained from the salt formation of dimethylamine and hydrochloric acid.

124-40-3
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506-59-2
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Yield:506-59-2 3 g

Reaction Conditions:

with hydrogenchloride in water at 0; for 0.5 h;

Steps:

Me2NH.HCl was prepared from aq dimethylamine solution (5.0 mL, 40%) by theaddition of conc. HCl (5.0 mL, 35%) at 0 C. The reaction mixture was stirred for0.5 h and then the water was evaporated. The solid fraction was azeotropedthrice with toluene to afford white solid compound (3.0 g), which was storedunder inert atmospher

References:

Khatik, Gopal L.;Sharma, Ratnesh;Kumar, Varun;Chouhan, Mangilal;Nair, Vipin A. [Tetrahedron Letters,2013,vol. 54,# 45,p. 5991 - 5993]

103-83-3 Synthesis