DIPYRIDIN-3-YLMETHANE synthesis
- Product Name:DIPYRIDIN-3-YLMETHANE
- CAS Number:78210-43-2
- Molecular formula:C11H10N2
- Molecular Weight:170.21
35779-35-2
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78210-43-2
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Yield:78210-43-2 96%
Reaction Conditions:
Stage #1: di-3-pyridylmethanonewith potassium hydroxide in ethylene glycol at 20; for 1 h;Inert atmosphere;Wolff-Kishner reduction;
Stage #2: with hydrazine hydrate at 185; for 1.75 h;Inert atmosphere;Wolff-Kishner reduction;
References:
Park, Byung Sun;Lee, Sang Woo;Kim, In Tae;Tae, Jin Sung;Lee, So Ha [Heteroatom Chemistry,2012,vol. 23,# 1,p. 66 - 73] Location in patent:experimental part
626-55-1
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93-60-7
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504-29-0
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737007-16-8
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