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ChemicalBook CAS DataBase List ethyl 2,2-difluorobut-3-enoate
60758-43-2

ethyl 2,2-difluorobut-3-enoate synthesis

4synthesis methods
Butanoic acid, 2,2-difluoro-3-(phenylsulfinyl)-, ethyl ester

185422-94-0
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ethyl 2,2-difluorobut-3-enoate

60758-43-2
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Yield:60758-43-2 77%

Reaction Conditions:

in neat (no solvent) at 120;

References:

Bildstein, Sylvia;Ducep, Jean-Bernard;Jacobi, Detlef [Tetrahedron Letters,1996,vol. 37,# 48,p. 8759 - 8762]