Ethyl 2-(4-cyanophenyl)acrylate synthesis
- Product Name:Ethyl 2-(4-cyanophenyl)acrylate
- CAS Number:409359-86-0
- Molecular formula:C12H11NO2
- Molecular Weight:201.23
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Yield:409359-86-0 97%
Reaction Conditions:
Stage #1: 2-bromo-acrylic acid ethyl esterwith naphthalene;tetraethylammonium perchlorate;zinc in N,N-dimethyl-formamide at -20; for 1 h;
Stage #2: 4-iodobenzonitrile;dichlorobis(tri-O-tolylphosphine)palladium in N,N-dimethyl-formamide at 70; for 3 h;
References:
Jalil;Kurono;Tokuda [Synlett,2001,# 12,p. 1944 - 1946]
5459-35-8
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623-00-7
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