ethyl 2-cyano-3-ethoxycrotonate synthesis

1synthesis methods

Product Name:ethyl 2-cyano-3-ethoxycrotonate
CAS Number:35260-93-6
Molecular formula:C9H13NO3
Molecular Weight:183.2

78-39-7 Synthesis

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105-56-6
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Yield: 79.5%

Reaction Conditions:

with acetic acid at 110 - 120; for 18 h;Inert atmosphere;Large scale;

References:

Fandrick, Daniel R.;Sanyal, Sanjit;Kaloko, Joseph;Mulder, Jason A.;Wang, Yuwen;Wu, Ling;Lee, Heewon;Roschangar, Frank;Hoffmann, Matthias;Senanayake, Chris H. [Organic Letters,2015,vol. 17,# 12,p. 2964 - 2967] Location in patent:supporting information

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