ETHYL 3-(6-CHLORO-3-PYRIDYL)-3-OXOPROPANOATE synthesis
- Product Name:ETHYL 3-(6-CHLORO-3-PYRIDYL)-3-OXOPROPANOATE
- CAS Number:216317-64-5
- Molecular formula:C10H10ClNO3
- Molecular Weight:227.64
Yield:216317-64-5 79%
Reaction Conditions:
Stage #1: 6-chloronicotinonitrile;ethyl bromoacetate in tetrahydrofuran at 60 - 120; for 0.166667 h;Flow reactor;Green chemistry;Blaise Reaction;
Stage #2: with hydrogenchloride in tetrahydrofuran; for 1 h;Green chemistry;
References:
Huck;Berton;De La Hoz;Díaz-Ortiz;Alcázar [Green Chemistry,2017,vol. 19,# 6,p. 1420 - 1424] Location in patent:supporting information
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