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ChemicalBook CAS DataBase List ETHYL 5-(3-METHOXYPHENYL)-5-OXOVALERATE
898751-99-0

ETHYL 5-(3-METHOXYPHENYL)-5-OXOVALERATE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: magnesium / tetrahydrofuran / -40 °C
1.2: 1.5 h / -40 °C
2.1: sulfuric acid / 7 h / Reflux

References:

Yang, Xiao-Hui;Xie, Jian-Hua;Liu, Wei-Peng;Zhou, Qi-Lin [Angewandte Chemie - International Edition,2013,vol. 52,# 30,p. 7833 - 7836][Angew. Chem.,2013,vol. 125,# 30,p. 7987 - 7990,4]

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