Hoechst 33342 synthesis
- Product Name:Hoechst 33342
- CAS Number:23491-52-3
- Molecular formula:C27H28N6O
- Molecular Weight:452.55
109-01-3
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23491-52-3
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 60 percent / K2CO3 / dimethylformamide / 4.5 h / Heating
2: H2 / 10percent Pd/C / methanol / 1.25 h / Ambient temperature
3: 1.171 g / AcOH / 12 h / 55 °C
4: H2 / 10percent Pd/C / methanol / 1.25 h / Ambient temperature
5: 80 percent / mol. sieves / nitrobenzene; toluene / 36 h / 98 - 100 °C
References:
Harapanhalli;McLaughlin;Howell;Rao;Adelstein;Kassis [Journal of medicinal chemistry,1996,vol. 39,# 24,p. 4804 - 4809]
10031-82-0
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23491-49-8
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23491-52-3
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1635-61-6
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23491-52-3
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23623-05-4
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23491-52-3
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6393-40-4
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$15.00/1g
23491-52-3
193 suppliers
$40.29/25mg