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16183-46-3

α-Hydroxybutyrophenone synthesis

10synthesis methods
-

Yield:16183-45-2 92%

Reaction Conditions:

with 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate;caesium carbonate in m-xylene at 20; for 24 h;Inert atmosphere;chemoselective reaction;

References:

Jin, Ming Yu;Kim, Sun Min;Mao, Hui;Ryu, Do Hyun;Song, Choong Eui;Yang, Jung Woon [Organic and Biomolecular Chemistry,2014,vol. 12,# 10,p. 1547 - 1550] Location in patent:supporting information