ISOPROPYLAMINE HYDROCHLORIDE synthesis
- Product Name:ISOPROPYLAMINE HYDROCHLORIDE
- CAS Number:15572-56-2
- Molecular formula:C3H10ClN
- Molecular Weight:95.57
75-31-0
15572-56-2
GENERAL PROCEDURE: Ammonium chloride (0.54 g, 10 mmol) and ethanol (3 mL) were added to a 25 mL round-bottom flask, followed by isopropylamine (10 mmol). The reaction mixture was placed on a magnetic stirrer and heated to reflux for 2 hours. After completion of the reaction, the solvent was removed by rotary evaporator to give propyl-2-amine hydrochloride as a solid in quantitative yield.
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Yield:15572-56-2 100%
Reaction Conditions:
with hydroxylamine hydrochloride in ethanol for 2 h;Reflux;
Steps:
General procedure for the preparation of amine hydrochloride salts 2c-2r
General procedure: To a 25-mL round-bottomed flask containing ammonium chloride (0.54 g, 10 mmol) was added ethanol (3 mL) followed by the requisite amine (10 mmol). The mixture was magnetically stirred and refluxed for 2 h. The solvent was then removed by rotary evaporation affording the hydrochloride salt as a solid invariably in quantitative yield.
References:
Di Grandi, Martin J.;Bennett, Caitlin;Cagino, Kristen;Muccini, Arnold;Suraci, Corey;Saba, Shahrokh [Synthetic Communications,2015,vol. 45,# 22,p. 2601 - 2607] Location in patent:supporting information
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