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ChemicalBook CAS DataBase List (+)-MAACKIAIN

(+)-MAACKIAIN synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 53 percent / PdCl2; LiCl / acetone / 2.5 h
2: 92 percent / H2 / Pd/C / acetone; tetrahydrofuran
3: 2 percent / DMAP / benzene / 15 h / Heating
4: LiAlH4 / diethyl ether; benzene / 0.33 h

References:

Tokes, Adrienne L.;Litkei, Gyoergy;Gulacsi, Katalin;Antus, Sandor;Baitz-Gacs, Eszter;Szantay, Csaba;Darko, Laszlo L. [Tetrahedron,1999,vol. 55,# 30,p. 9283 - 9296]