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ChemicalBook CAS DataBase List Methoxy(4-methoxyphenyl)dimethylsilane
62244-48-8

Methoxy(4-methoxyphenyl)dimethylsilane synthesis

5synthesis methods
-

Yield:62244-48-8 80%

Reaction Conditions:

Product distribution / selectivity;Electrochemical reaction;

Steps:

7 Synthesis of (p-methoxyphenyl)methoxydimethylsilane

EXAMPLE 7 Synthesis of (p-methoxyphenyl)methoxydimethylsilane 5.00 g (35.1 mmol) of p-chloranisole and 4.22 g (35.1 mmol) of dimethoxydimethylsilane are reacted with one another electrochemically in a similar manner to example 1. After a total electrolysis time of 138 h (amount of charge Q=2.2 F/mol) and similar workup to example 1, 5.50 g of the product, p-methoxyphenylmethoxydimethylsilane, are obtained (yield: 80% of theory).

References:

US2005/234255,2005,A1 Location in patent:Page/Page column 4

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