Methyl 1-(Mercaptomethyl)cyclopropaneacetate synthesis
- Product Name:Methyl 1-(Mercaptomethyl)cyclopropaneacetate
- CAS Number:152922-73-1
- Molecular formula:C7H12O2S
- Molecular Weight:160.23
67-56-1
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![2-[1-(Mercaptomethyl)cyclopropyl]acetic acid](/CAS/GIF/162515-68-6.gif)
162515-68-6
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152922-73-1
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Yield:-
Reaction Conditions:
with thionyl chloride at 0 - 65;
Steps:
1
Example 1: Preparation of methyl ester of l-(mercaptomethyl) cyclopropane acetic acid; Thionyl chloride (7.4 ml) was added to solution of l-(mercaptomethyl) cyclopropane acetic acid (10.0 gm) in methanol (100 ml) at 0-5°C. The reaction mixture thus obtained was stirred at 60-650C for 2 hours and concentrated under reduced pressure^ to get methyl ester of 1 -(mercaptomethyl) cyclopropane acetic acid. Yield: 9.0 gm
References:
MACLEODS PHARMACEUTICALS LIMITED WO2009/138993, 2009, A1 Location in patent:Page/Page column 13
67-56-1
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$7.29/5ml-f
152922-72-0
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152922-73-1
135 suppliers
$45.00/500mg