METHYL 2,3,4,6-TETRA-O-BENZYL-Α-D-MANNOPYRANOSIDE synthesis
- Product Name:METHYL 2,3,4,6-TETRA-O-BENZYL-Α-D-MANNOPYRANOSIDE
- CAS Number:83462-67-3
- Molecular formula:C35H38O6
- Molecular Weight:554.67
Yield:83462-67-3 73.3%
Reaction Conditions:
Stage #1: methyl-α,β-D-mannopyranosidewith sodium hydride in N,N-dimethyl-formamide;mineral oil at 0;
Stage #2: benzyl chloridewith tetra-(n-butyl)ammonium iodide in N,N-dimethyl-formamide;mineral oil at 0 - 20;
References:
Voshavar, Chandrashekhar;Meka, Rakesh C. R.;Samanta, Sanjoy;Marepally, Srujan;Chaudhuri, Arabinda [Journal of Medicinal Chemistry,2017,vol. 60,# 4,p. 1605 - 1610] Location in patent:supporting information
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