METHYLTRIOXORHENIUM(VII) synthesis
- Product Name:METHYLTRIOXORHENIUM(VII)
- CAS Number:70197-13-6
- Molecular formula:CH3O3Re
- Molecular Weight:249.24
10466-65-6
117 suppliers
$15.90/0.2g
594-27-4
120 suppliers
$28.00/5g
70197-13-6
138 suppliers
$30.69/100mg
Yield:70197-13-6 63%
Reaction Conditions:
with chloro-trimethyl-silane;sulfuric acid in acetonitrile(hood); stirring (25°C, 24 h); evapn. (reduced pressure), extn. (n-pentane), concn., standing (-35°C, 24 h), purifn. by sublimation (25°C/E-2 mbar);
References:
Herrmann;Kratzer;Fischer [Angewandte Chemie - International Edition in English,1997,vol. 36,# 23,p. 2652 - 2654]