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N-4-Pyridylbenzenesulfonamide synthesis

2synthesis methods
-

Yield:15309-85-0 90%

Reaction Conditions:

with (1,2-dimethoxyethane)dichloronickel(II);bis(2-phenylpyridinato)(2,2'-bipyridine)iridium(III) hexafluorophosphate;N,N,N',N'-tetramethylguanidine in acetonitrile at 35; for 8 h;Inert atmosphere;Irradiation;Glovebox;Temperature;

References:

Kim, Taehoon;McCarver, Stefan J.;Lee, Chulbom;MacMillan, David W. C. [Angewandte Chemie - International Edition,2018,vol. 57,# 13,p. 3488 - 3492][Angew. Chem.,2018,vol. 130,p. 3546 - 3550,5] Location in patent:supporting information