N-Cyclohexyl-2-benzothiazolesulfenamide synthesis
11synthesis methods
- Product Name:N-Cyclohexyl-2-benzothiazolesulfenamide
- CAS Number:95-33-0
- Molecular formula:C13H16N2S2
- Molecular Weight:264.41
Yield:95-33-0 96%
Reaction Conditions:
with oxygen in water at 60; under 3000.3 Torr; for 4 h;Autoclave;
Steps:
1-8 Specific example 8:
2 mmol of 2-mercaptobenzothiazole, 8 mmol of cyclohexylamine, 1 wt% of cobalt catalyst, 8 mL of water were added to a high-pressure reaction kettle, and oxygen was passed in until the pressure stabilized at 0.4 MPa and heated in an oil bath At 60 ° C. for 4 h, a white solid was formed, filtered, washed, and dried, and the yield was 96%.
References:
Liaocheng University;Huang Xianqiang;Qi Yuquan;Zhao Wenli;Li Chunxia;Zheng Jun;Liu Sen;Gu Xiaoyu CN110305075, 2019, A Location in patent:Sheet 0021-0028
