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144697-33-6

N-ETHYLIDENEETHYLENEDIAMINE synthesis

3synthesis methods
-

Yield:1001-53-2 14 %Spectr. ,144697-33-6 47 %Spectr.

Reaction Conditions:

with (6-di-tert-butylphosphinomethyl-2,2’-bipyridyl)Ru(CO)HCl;potassium tert-butylate;hydrogen in ethanol at 115; under 37503.8 Torr; for 48 h;

References:

Hu, Peng;Ben-David, Yehoshoa;Milstein, David [Angewandte Chemie - International Edition,2016,vol. 55,# 3,p. 1061 - 1064][Angew. Chem.,2016,vol. 128,# 3,p. 1073 - 1076,4] Location in patent:supporting information