N-tert-Butyl-2-benzothiazolesulfenamide synthesis
- Product Name:N-tert-Butyl-2-benzothiazolesulfenamide
- CAS Number:95-31-8
- Molecular formula:C11H14N2S2
- Molecular Weight:238.37
Yield:95-31-8 98.4%
Reaction Conditions:
with sodium hypochlorite at 40; for 0.166667 h;Temperature;
Steps:
4 Example 4:
Weigh 50g accelerator M 220g of tert-butylamine formulated into a solution,Then take 180g of sodium hypochlorite (effective chlorine content of 13%),Through the flow pump driven two-phase solution through the Y mixer into the plate diameter of 1mm reactor,The flow rate of the microreactor was 0.5 mL / min, the residence time of the reaction liquid in the reactor was 10 min,The reaction temperature is 40 ° C.After one cycle, collect the reaction solution. After testing to determine the yield was 98.4%105.0 ° C melting point,Appearance is white powder.
References:
Shandong Sidier Chemical Technology Co., Ltd.;Zhu Jiazhen;Wang Jincai;Tian Xu;Zhao Xinyuan;Wang Ying CN106866578, 2017, A Location in patent:Paragraph 0021; 0022; 0023; 0024; 0025
149-30-4
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95-31-8
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