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ChemicalBook CAS DataBase List Norbornene
498-66-8

Norbornene synthesis

4synthesis methods
Continuous production using two kettle reactors in series:
Reactor 1 (170-190°C, 7-11 MPa): Dicyclopentadiene (DCPD) cracks to cyclopentadiene (CPD) in solvent MIBK and undergoes Diels-Alder reaction with ethylene to form norbornene (NB).
Reactor 2
-

Yield:498-66-8 80%

Reaction Conditions:

with disodium hydrogenphosphate;sodium amalgam in tetrahydrofuran;methanol; for 11 h;

References:

Carr, Richard V. C.;Williams, Richard V.;Paquette, Leo A. [Journal of Organic Chemistry,1983,vol. 48,# 25,p. 4976 - 4986]

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