(R)-(4-Methoxyphenyl)oxirane synthesis
- Product Name:(R)-(4-Methoxyphenyl)oxirane
- CAS Number:62600-73-1
- Molecular formula:C9H10O2
- Molecular Weight:150.17
117465-37-9
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62600-73-1
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Yield:62600-73-1 95%
Reaction Conditions:
with sodium hydroxide in tetrahydrofuran;water at 20; for 1 h;enantioselective reaction;
Steps:
General procedure for the synthesis of chiral styrene oxides
General procedure: For the preparation of chiral styrene oxides, 3 mL NaOH(2 N) was added to α-bromohydrin (0.5 mmol) in 6 mL tetrahydrofuran(THF) and then was sttired at room temperature for 1 h. After completing the reaction, the product was extracted by EtOAc and then purified using column chromatography on silica gel using ethyl acetate/n-hexane gradient to give the desired product in high purity.
References:
Hosseinzadeh, Rahman;Mohadjerani, Maryam;Mesgar, Sakineh [Journal of the Iranian Chemical Society,2019,vol. 16,# 3,p. 583 - 591]
2632-13-5
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$5.00/25mg
62600-73-1
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![Benzenemethanol, α-[[(R)-butylsulfinyl]methyl]-4-methoxy-, (αR)-](/CAS/20210305/GIF/1190369-08-4.gif)
1190369-08-4
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62600-73-1
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