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tert-butyl 4-(dimethylamino)-4-oxobutylcarbamate synthesis

3synthesis methods
-

Yield:154656-95-8 31%

Reaction Conditions:

with [Ir(5-(trifluoromethyl)-2-(2,4-difluorophenyl)pyridine)2(2,2'-bipyridine)](PF6) in methanol;acetone at 20; for 4 h;Schlenk technique;Inert atmosphere;Irradiation;

References:

Miyazawa, Kazuki;Koike, Takashi;Akita, Munetaka [Advanced Synthesis and Catalysis,2014,vol. 356,# 13,p. 2749 - 2755]