Tetraethyl (1,6-hexylene)bisphosphonate synthesis
- Product Name:Tetraethyl (1,6-hexylene)bisphosphonate
- CAS Number:5391-92-4
- Molecular formula:C14H32O6P2
- Molecular Weight:358.35
Yield:5391-92-4 96%
Reaction Conditions:
Stage #1: phosphonic acid diethyl esterwith sodium in acetonitrile;Inert atmosphere;Michaelis-Becker reaction;
Stage #2: 1 ,6-dibromohexane in acetonitrile; for 0.0333333 h;Inert atmosphere;Microwave irradiation;Michaelis-Becker reaction;
References:
Meziane, Dalila;Hardouin, Julie;Elias, Abdelhamid;Guenin, Erwann;Lecouvey, Marc [Heteroatom Chemistry,2009,vol. 20,# 6,p. 369 - 377] Location in patent:experimental part
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