ChemicalBook CAS DataBase List Z-ILE-VAL-OH

Z-ILE-VAL-OH synthesis

6synthesis methods

Product Name:Z-ILE-VAL-OH
CAS Number:41487-00-7
Molecular formula:C19H28N2O5
Molecular Weight:364.44

72-18-4 Synthesis

72-18-4
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 85 percent / thionylchloride / Ambient temperature
2: 85 percent / triethylamine, chloroformic acid ethyl ester / CH₂Cl₂ / 1) -10 deg C, 1 h, 2) 2 h, room temperature
3: NaI / acetone
4: Zn, HgCl₂ / acetone / 48 h / Heating

References:

Buchholz, Michael;Kunz, Horst [Liebigs Annalen der Chemie,1983,# 11,p. 1859 - 1885]

72-18-4 Synthesis

72-18-4
805 suppliers
$5.00/25g