3,5-dichloro-N-phenylBenzenamine synthesis
- Product Name:3,5-dichloro-N-phenylBenzenamine
- CAS Number:105836-68-8
- Molecular formula:C12H9Cl2N
- Molecular Weight:238.11
39943-56-1
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Yield:105836-68-8 70%
Reaction Conditions:
Stage #1: anilinewith copper diacetate in acetonitrile at -5; for 0.25 h;
Stage #2: with 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile at -5; for 0.0833333 h;
Stage #3: 3,5-dichlorophenylhydrazine in acetonitrile at -5; for 3.33333 h;
References:
Jadhav, Ravindra R.;Huddar, Sameerana N.;Akamanchi, Krishnacharya G. [European Journal of Organic Chemistry,2013,# 30,p. 6779 - 6783] Location in patent:supporting information
626-43-7
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