4-(BENZYLTHIO)PHENOL synthesis

9synthesis methods

Product Name:4-(BENZYLTHIO)PHENOL
CAS Number:30519-03-0
Molecular formula:C13H12OS
Molecular Weight:216.3

637-89-8 Synthesis

637-89-8
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100-44-7 Synthesis

100-44-7
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30519-03-0
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$110.00/50mg

Yield:30519-03-0 96%

Reaction Conditions:

with triethylamine in chloroform; for 8 h;Reflux;

Steps:

1.1 Preparation of 1,4- (Benzylthio) phenol:

12.6 g (0.1 mol) of 4-mercaptophenol and 12.12 g (0.12 mol) of triethylamine were added to a three-necked reaction flask equipped with a thermometer and an electric stirrer, and 12.6 (0.1 mol) of benzyl chloride 100ml of chloroform solution, dropping time is 2h. Then heated to reflux for 6 h. After completion of the reaction, poured into 150ml of water, the separation of several layers, washed with 3 × 100ml of water, anhydrous sodium sulfate and concentrated to a yellow solid 4- (benzylthio) phenol, and then recrystallization from anhydrous methanol, yellow Solid 20.7 g Yield 96%

References:

CN105541686,2016,A Location in patent:Paragraph 0023; 0026; 0027; 0028

637-89-8 Synthesis

637-89-8
166 suppliers
$24.00/5g