ChemicalBook--->CAS DataBase List--->10397-30-5

10397-30-5

10397-30-5 Structure

10397-30-5 Structure
IdentificationMore
[Name]

4-Methyl-3-nitrobenzoyl chloride
[CAS]

10397-30-5
[Synonyms]

3-NITRO-4-METHYLBENZOYLCHLORIDE
3-NITRO-P-TOLUOYL CHLORIDE
3-NITRO-P-TOLUYL CHLORIDE
4-METHYL-3-NITROBENZOYL CHLORIDE
TIMTEC-BB SBB007967
Benzoyl chloride, 4-methyl-3-nitro-
4-METHYL-3-NITROBENZOYL CHLORIDE/3-NITRO-P-TOLUYL CHLORIDE
4-METHYL-3-NITROBENZOYL CHLORIDE 99%
[EINECS(EC#)]

233-858-1
[Molecular Formula]

C8H6ClNO3
[MDL Number]

MFCD00035747
[Molecular Weight]

199.59
[MOL File]

10397-30-5.mol
Chemical PropertiesBack Directory
[Melting point ]

20-21 °C(lit.)
[Boiling point ]

185 °C36 mm Hg(lit.)
[density ]

1.37 g/mL at 25 °C(lit.)
[refractive index ]

n20/D 1.581(lit.)
[Fp ]

>230 °F
[form ]

liquid
[CAS DataBase Reference]

10397-30-5(CAS DataBase Reference)
[NIST Chemistry Reference]

4-Methyl-3-nitrobenzoyl chloride(10397-30-5)
Safety DataBack Directory
[Hazard Codes ]

C
[Risk Statements ]

R34:Causes burns.
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S27:Take off immediately all contaminated clothing .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
[RIDADR ]

UN 3265 8/PG 2
[WGK Germany ]

3
[HS Code ]

2916399090
Hazard InformationBack Directory
[Uses]

4-Methyl-3-nitrobenzoyl chloride was used in the synthesis of 4-amino-1,5-naphthalenedisulphonate acid monosodium salt, an intermediate employed in the synthesis of modified suramin molecule.
It may be used in the synthesis of the following:
  • benzophenone derivative
  • substituted 3-amino-4-methyl-N-phenylbenzamide
  • retroamide
  • 4-methyl-3-nitro-N-phenylbenzamide
[General Description]

4-Methyl-3-nitrobenzoyl chloride is a benzoyl chloride derivative. It has been reported to be synthesized from 4-methyl-3-nitrobenzoic acid.
[Purification Methods]

Recrystallise the acid from EtOH. The S-benzylisothiuronium salt has m 167-168o (EtOH). The acid chloride [10397-30-5] has m 20-21o, b 185o/36mm, and the methyl ester [7356-11-8] crystallises as pale yellow needles from MeOH with m 51o. [Beilstein 9 H 502, 9 II 334, 9 III 2359.]
Spectrum DetailBack Directory
[Spectrum Detail]

4-Methyl-3-nitrobenzoyl chloride(10397-30-5)IR
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

10397-30-5(sigmaaldrich)
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