ChemicalBook--->CAS DataBase List--->206559-43-5

206559-43-5

206559-43-5 Structure

206559-43-5 Structure
IdentificationMore
[Name]

5-BROMO-2-IODO-M-XYLENE
[CAS]

206559-43-5
[Synonyms]

5-BROMO-2-IODO-1,3-XYLENE
5-BROMO-2-IODO-3-XYLENE
5-BROMO-2-IODO-M-XYLENE
[EINECS(EC#)]

606-594-3
[Molecular Formula]

C8H8BrI
[MDL Number]

MFCD03094656
[Molecular Weight]

310.96
[MOL File]

206559-43-5.mol
Chemical PropertiesBack Directory
[Melting point ]

42 °C
[Boiling point ]

282℃
[density ]

1.940
[Fp ]

125℃
[storage temp. ]

Keep in dark place,Sealed in dry,2-8°C
[form ]

fused solid
[color ]

Faint peach
[CAS DataBase Reference]

206559-43-5(CAS DataBase Reference)
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)
GHS07
[Signal word ]

Warning
[Hazard statements ]

H315-H319-H335
[Precautionary statements ]

P271-P261-P280
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
[Hazard Note ]

Irritant
[HazardClass ]

IRRITANT
[HS Code ]

2903998090
Spectrum DetailBack Directory
[Spectrum Detail]

5-BROMO-2-IODO-M-XYLENE(206559-43-5)1HNMR
5-BROMO-2-IODO-M-XYLENE(206559-43-5)FT-IR
Hazard InformationBack Directory
[Synthesis]

4-Bromo-2,6-dimethylaniline

24596-19-8

5-BROMO-2-IODO-M-XYLENE

206559-43-5

The diazotization reaction was carried out using sodium nitrite and hydrochloric acid in acetonitrile solvent at 0 °C using 4-bromo-2,6-dimethylaniline as starting material. Subsequently, the diazonium group was converted to iodine by addition of potassium iodide to afford the target product 5-bromo-2-iodo-1,3-xylene in 96% yield. The synthesis was described with reference to known literature (NonPatentDocument 2).

[References]

[1] Journal of Medicinal Chemistry, 2018, vol. 61, # 16, p. 7202 - 7217
[2] Patent: JP5959171, 2016, B2. Location in patent: Paragraph 0258-0260
[3] Bulletin of the Chemical Society of Japan, 2001, vol. 74, # 11, p. 2207 - 2218
[4] Patent: WO2009/74314, 2009, A1. Location in patent: Page/Page column 168-169
206559-43-5 suppliers list
Company Name: J & K SCIENTIFIC LTD.  
Telephone: 18210857532 18210857532
Website: https://www.jkchemical.com
Company Name: PharmaBlock Sciences (Nanjing),Inc.  
Telephone: 025-86918202 4000255188
Website: http://www.pharmablock.com/
Company Name: BeiJing Hwrk Chemicals Limted  
Telephone: 0757-86329057 18934348241
Website: www.hwrkchemical.com/
Company Name: Energy Chemical  
Telephone: 400-0056266
Website: www.energy-chemical.com
Company Name: Wuhan Chemwish Technology Co., Ltd  
Telephone: 86-027-67849912
Website: www.chemwish.com
Company Name: Capot Chemical Co., Ltd  
Telephone: +86 (0) 571 85 58 67 18
Website: www.capotchem.com
Company Name: Shanghai Sinch Parmaceuticals Tech. Co. Ltd.  
Telephone: +86-21-54098501
Website: www.sinch.com.cn
Company Name: Jia Xing Isenchem Co.,Ltd  
Telephone: 0573-85285100 18627885956
Website: https://www.chemicalbook.com/ShowSupplierProductsList14265/0_EN.htm
Company Name: Accela ChemBio Co.,Ltd.  
Telephone: 4000665055
Website: www.shao-yuan.com/
Company Name: Nanjing Chemlin Chemical Co., Ltd  
Telephone: 025-83697070 13770331960
Website: www.echemlin.cn
Company Name: Shanghai Hanhong Scientific Co.,Ltd.  
Telephone: 021-54306202 13764082696
Website: https://www.hanhongsci.com
Company Name: Hangzhou Dingxin Biotechnology Co., Ltd.  
Telephone: 0571-88194596 15558156576
Website: http://www.hzdxbio.com/
Company Name: Aemon Chemical  
Telephone: 0086-755-86198205
Website: www.aemonchem.com
Company Name: Shanghai Topbiochem Technology Co., Ltd  
Telephone: +86-21-60341587
Website: www.topbiochem.com
Company Name: Shanghai Jian Chao Chemical Technology Co., Ltd.  
Telephone: 150-2103-5486 18017383231
Website:
Company Name: 9ding chemical ( Shanghai) Limited  
Telephone: 4009209199
Website: www.9dingchem.com
Company Name: Shanghai Aladdin Bio-Chem Technology Co.,LTD  
Telephone: 400-6206333 13167063860
Website: www.aladdin-e.com/
Company Name: Shanghai Yolne Chemical Co., Ltd.  
Telephone: 021-62960152
Website: http://www.yolne.com
Tags:206559-43-5 Related Product Information
7783-96-2 7789-33-5 116632-39-4 206559-43-5 108-38-3 589-87-7