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33024-60-1

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33024-60-1 Structure

33024-60-1 Structure
IdentificationMore
[Name]

4-Aminotetrahydropyran hydrochloride
[CAS]

33024-60-1
[Synonyms]

4-AMINOTETRAHYDRO-4H-PYRAN HYDROCHLORIDE
4-AMINOTETRAHYDROPYRAN, HCL
4-AMINOTETRAHYDROPYRAN HYDROCHLORIDE
ATHP-HCL
TETRAHYDRO-PYRAN-4-YLAMINE HYDROCHLORIDE
4-AMINOTETRAHYDROPYRAN HYDROCHLORIDE (TETRAHYDRO-2H-PYRAN-4-AMINE HYDROCHLORIDE)
Tetrahydro-2H-pyran-4-amine hydrochloride
4-Aminotetrahydro-2H-pyran hydrochloride
TETRAHYDRO-PYRAN-4-YLAMINE HCL
[Molecular Formula]

C5H12ClNO
[MDL Number]

MFCD00100881
[Molecular Weight]

137.61
[MOL File]

33024-60-1.mol
Chemical PropertiesBack Directory
[Melting point ]

230-250°C
[storage temp. ]

Keep Cold
[form ]

crystalline powder
[color ]

white
[InChI]

InChI=1S/C5H11NO.ClH/c6-5-1-3-7-4-2-5;/h5H,1-4,6H2;1H
[InChIKey]

KWZSCXIYGVEHOB-UHFFFAOYSA-N
[SMILES]

C1(N)CCOCC1.Cl
[CAS DataBase Reference]

33024-60-1(CAS DataBase Reference)
Questions And AnswerBack Directory
[Uses]

4-Aminotetrahydropyran hydrochloride is an organic heterocyclic compound that can be used as a pharmaceutical intermediate.
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)
GHS07
[Signal word ]

Warning
[Hazard statements ]

H315-H319-H335
[Precautionary statements ]

P261-P271-P280
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
[WGK Germany ]

WGK 3
[Hazard Note ]

Harmful/Irritant/Keep Cold
[HazardClass ]

IRRITANT
[HS Code ]

2932209090
[Storage Class]

11 - Combustible Solids
[Hazard Classifications]

Acute Tox. 4 Oral
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Tetrahydrofuran-->Lithium Aluminum Hydride-->Hydroxylamine hydrochloride-->Sodium acetate-->tert-Butyl methyl ether-->Tetrahydro-4H-pyran-4-one-->2H-Pyran-4-amine, tetrahydro-N,N-bis(phenylmethyl)--->4-Aminotetrahydropyran-->Tetrahydro-pyran-4-one oxime-->Tetrahydro-2H-pyran-4-carboxylic acid
[Preparation Products]

Gilteritinib
Spectrum DetailBack Directory
[Spectrum Detail]

4-Aminotetrahydropyran hydrochloride(33024-60-1)1HNMR
Hazard InformationBack Directory
[Synthesis]

A mixture of 4-(hydroxyimino)-3,5,6-trihydro-2H-pyran (43.4 mmol) and Raney Nickel (200 mg) in ethanol was hydrogenated (90 psi) at room temperature for 3 days. The mixture was filtered through a pad of Celite, washed with MeOH, and concentrated. The residue was dissolved in MeOH, treated with HCl (4 N in dioxane, 60 mmol), and concentrated to give perhydro-2H-pyran-4-ylamine hydrochloride (4-Aminotetrahydropyran hydrochloride).
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