| Identification | Back Directory | [Name]
(2-METHYL-PYRIDIN-3-YL)-METHANOL | [CAS]
56826-61-0 | [Synonyms]
2-Methyl-3-PyridineMethanol
3-(HYDROXYMETHYL)-A-PICOLINE
3-Pyridinemethanol, 2-methyl-
(2-Methylpyridine-3-yl)Methanol
(2-METHYL-PYRIDIN-3-YL)-METHANOL
3-(HYDROXYMETHYL)-ALPHA-PICOLINE
3-Hydroxymethyl-2-methylpyridine
(2-Mehtyl-pyridin-3-yl)-methanol
3-METHYL-3-HYDROXYMETHYL PYRIDINE
2-METHYL-3-HYDROXYMETHYL PYRIDINE
2-Methyl-3-hydroxyMethyl pyridine 97%
(2-METHYL-PYRIDIN-3-YL)-METHANOL ISO 9001：2015 REACH
3-Hydroxymethyl-2-methylpyridine
(2-Methylpyridin-3-yl)methanol | [EINECS(EC#)]
627-573-5 | [Molecular Formula]
C7H9NO | [MDL Number]
MFCD00030820 | [MOL File]
56826-61-0.mol | [Molecular Weight]
123.15 |
| Chemical Properties | Back Directory | [Boiling point ]
262 °C (lit.) | [density ]
1.106 g/mL at 25 °C (lit.) | [refractive index ]
n20/D 1.545(lit.) | [Fp ]
>230 °F | [storage temp. ]
Inert atmosphere,Room Temperature | [Appearance]
Light yellow to yellow Solid-liquid mixture |
| Hazard Information | Back Directory | [Chemical Properties]
light yellow oil liquid | [Synthesis]
A solution of methyl 2-methylnicotinate (35.2 g, 234 mmol) in 275 ml of dry ether was added dropwise to a vigorously stirred suspension of LiAlH4 (13.3 g, 350 mmol) in 600 ml of anhydrous ether. The reaction mixture was heated and refluxed in an oil bath at 55°C for 1.5 h and subsequently cooled to 0°C. H2O (64 ml) was added slowly dropwise, and the reaction was carried out for 1 h. The supernatant was decanted. The remaining suspension was extracted with ether. All organic phases were combined, dried over MgSO4 and the solvent was evaporated to give 29.9 g (234 mmol, 100% yield) of 3-(hydroxymethyl)-2-methylpyridine, the product being an orange-colored oil; GC analysis showed 100% purity. | [References]
[1] Patent: US2002/49316, 2002, A1
[2] Patent: US2005/124586, 2005, A1. Location in patent: Page/Page column 9-10
[3] Patent: WO2009/147211, 2009, A1. Location in patent: Page/Page column 25
[4] Patent: WO2009/42694, 2009, A1. Location in patent: Page/Page column 75
[5] Patent: US2004/6114, 2004, A1. Location in patent: Page 71 |
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| Company Name: |
Energy Chemical
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| Tel: |
021-021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
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