Cyclohexylthiophthalimide(17796-82-6) IR1
Product NameCyclohexylthiophthalimide
CAS17796-82-6
Molecular FormulaC14H15NO2S
Molecular Weight261.34
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MassMS-IW-8675 n-(cyclohexylthio)phthalimide C14H15NO2S (Mass of molecular ion: 261)
Source Temperature: 160 °C Sample Temperature: 130 °C Direct, 75 eV
27.0 1.8 29.0 2.6 39.0 3.5 41.0 13.7 43.0 1.0 45.0 1.8 50.0 2.8 53.0 2.2 54.0 2.4 55.0 28.4 56.0 1.5 67.0 7.5 71.0 1.4 73.0 1.0 75.0 1.4 76.0 8.4 77.0 2.1 79.0 2.3 80.0 3.3 81.0 11.3 82.0 3.4 83.0 12.3 84.0 1.0 85.0 1.1 102.0 1.2 104.0 9.3 105.0 1.1 114.0 63.9 115.0 4.9 116.0 3.1 130.0 7.5 136.0 2.4 147.0 2.3 148.0 8.3 151.0 6.6 162.0 1.1 178.0 1.0 179.0 100.0 180.0 31.4 181.0 7.5 182.0 1.6 228.0 9.7 229.0 1.5 261.0 7.0 262.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H15 N O2 S 0.040 g : 0.5 ml CDCl3 N-(cyclohexylthio)phthalimide 
Assign. Shift(ppm)
A 7.938 B 7.803 C 3.187 D 1.913 E 1.797 F 1.622 G 1.37 J 1.28 to 1.24
Hz ppm Int.3182.50 7.964 51 3181.03 7.960 61 3177.25 7.951 759 3174.19 7.943 758 3171.75 7.937 629 3168.70 7.929 1000 3164.79 7.919 105 3163.57 7.916 92 3126.95 7.825 87 3125.85 7.822 103 3124.63 7.819 38 3121.95 7.812 969 3118.90 7.805 628 3116.46 7.798 707 3113.28 7.791 765 3110.96 7.785 39 3109.62 7.781 77 3108.15 7.778 61 1288.45 3.224 54 1284.91 3.216 116 1281.37 3.207 72 1277.71 3.198 107 1274.05 3.188 222 1270.51 3.180 132 1266.85 3.170 60 1263.18 3.161 111 1259.52 3.152 69 770.87 1.929 183 766.97 1.920 127 765.87 1.917 106 760.62 1.904 197 758.54 1.899 207 758.06 1.897 207 726.81 1.819 128 724.37 1.813 156 721.19 1.805 155 714.97 1.789 208 711.18 1.780 202 707.28 1.770 98
in CDCl3
KBr disc
nujol mull
