Cyclohexylthiophthalimide(17796-82-6) IR2

Product NameCyclohexylthiophthalimide

CAS 17796-82-6

Molecular FormulaC14H15NO2S

Molecular Weight261.34

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Mass

MS-IW-8675          
n-(cyclohexylthio)phthalimide
C14H15NO2S          (Mass of molecular ion:    261)

   Source Temperature: 160 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      27.0       1.8
      29.0       2.6
      39.0       3.5
      41.0      13.7
      43.0       1.0
      45.0       1.8
      50.0       2.8
      53.0       2.2
      54.0       2.4
      55.0      28.4
      56.0       1.5
      67.0       7.5
      71.0       1.4
      73.0       1.0
      75.0       1.4
      76.0       8.4
      77.0       2.1
      79.0       2.3
      80.0       3.3
      81.0      11.3
      82.0       3.4
      83.0      12.3
      84.0       1.0
      85.0       1.1
     102.0       1.2
     104.0       9.3
     105.0       1.1
     114.0      63.9
     115.0       4.9
     116.0       3.1
     130.0       7.5
     136.0       2.4
     147.0       2.3
     148.0       8.3
     151.0       6.6
     162.0       1.1
     178.0       1.0
     179.0     100.0
     180.0      31.4
     181.0       7.5
     182.0       1.6
     228.0       9.7
     229.0       1.5
     261.0       7.0
     262.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₅ N O₂ S	0.040 g : 0.5 ml CDCl₃
N-(cyclohexylthio)phthalimide

    Assign.     Shift(ppm)

      A             7.938
      B             7.803
      C             3.187
      D             1.913
      E             1.797
      F             1.622
      G             1.37
      J          1.28 to 1.24

     Hz     ppm     Int.

   3182.50   7.964     51
   3181.03   7.960     61
   3177.25   7.951    759
   3174.19   7.943    758
   3171.75   7.937    629
   3168.70   7.929   1000
   3164.79   7.919    105
   3163.57   7.916     92
   3126.95   7.825     87
   3125.85   7.822    103
   3124.63   7.819     38
   3121.95   7.812    969
   3118.90   7.805    628
   3116.46   7.798    707
   3113.28   7.791    765
   3110.96   7.785     39
   3109.62   7.781     77
   3108.15   7.778     61
   1288.45   3.224     54
   1284.91   3.216    116
   1281.37   3.207     72
   1277.71   3.198    107
   1274.05   3.188    222
   1270.51   3.180    132
   1266.85   3.170     60
   1263.18   3.161    111
   1259.52   3.152     69
    770.87   1.929    183
    766.97   1.920    127
    765.87   1.917    106
    760.62   1.904    197
    758.54   1.899    207
    758.06   1.897    207
    726.81   1.819    128
    724.37   1.813    156
    721.19   1.805    155
    714.97   1.789    208
    711.18   1.780    202
    707.28   1.770     98

in CDCl3