3,4-Dichlorophenylhydrazine hydrochloride(19763-90-7) MS
Product Name3,4-Dichlorophenylhydrazine hydrochloride
CAS19763-90-7
Molecular FormulaC6H7Cl3N2
Molecular Weight213.49
InChIInChI=1S/C6H6Cl2N2.ClH/c7-5-2-1-4(10-9)3-6(5)8;/h1-3,10H,9H2;1H
InChIKey WIKZRYSGQPZTMM-UHFFFAOYSA-N
SmilesC1(NN)=CC=C(Cl)C(Cl)=C1.Cl
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MassMS-KW-0850 (3,4-dichlorophenyl)hydrazine hydrochloride C6H6Cl2N2 HCl (Mass of molecular ion: 176)
Source Temperature: 160 °C Sample Temperature: 130 °C Direct, 75 eV
17.0 2.5 18.0 8.0 28.0 5.2 29.0 6.6 30.0 1.6 31.0 4.0 35.0 6.0 36.0 54.2 37.0 4.6 38.0 19.5 39.0 2.0 44.5 3.0 49.0 2.8 50.0 5.3 51.0 4.1 52.0 3.8 60.0 1.0 61.0 4.2 62.0 7.2 62.5 2.1 63.0 9.5 64.0 2.3 70.0 1.6 71.0 1.1 72.0 2.7 73.0 9.2 74.0 10.7 75.0 16.6 76.0 2.6 77.0 5.5 78.0 2.6 83.0 1.6 84.0 2.8 85.0 3.5 86.0 1.8 87.0 1.9 88.0 7.7 89.0 5.2 90.0 5.4 97.0 5.6 98.0 2.4 99.0 4.1 105.0 1.3 107.0 1.8 109.0 8.8 110.0 2.5 111.0 17.0 112.0 3.7 113.0 4.9 114.0 2.5 124.0 17.8 125.0 18.3 126.0 8.5 127.0 6.2 133.0 25.7 134.0 2.3 135.0 16.3 136.0 1.2 137.0 2.9 141.0 16.0 142.0 1.9 143.0 5.0 145.0 7.0 146.0 11.1 147.0 6.9 148.0 7.6 149.0 2.4 150.0 1.7 159.0 10.0 160.0 59.5 161.0 21.6 162.0 39.3 163.0 11.3 164.0 7.1 165.0 1.6 174.0 2.4 175.0 3.1 176.0 100.0 177.0 8.9 178.0 62.0 179.0 5.0 180.0 10.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H6 Cl2 N2 0.039 g : 0.5 ml DMSO-d6 (3,4-dichlorophenyl)hydrazine hydrochloride 
Assign. Shift(ppm)
A 10.6 B 8.8 C 7.517 D 7.311 E 7.021
Hz ppm Int.4242.68 10.616 206 3524.67 8.820 26 3008.69 7.529 681 3004.48 7.518 51 2999.90 7.507 753 2995.32 7.495 24 2994.96 7.494 23 2923.34 7.315 940 2920.59 7.308 1000 2811.61 7.036 541 2808.86 7.029 518 2806.11 7.022 55 2805.56 7.021 54 2802.81 7.014 511 2800.07 7.007 503
in DMSO-d6
KBr disc
nujol mull
