4'-Chloro-3'-nitroacetophenone(5465-65-6) IR2

Product Name4'-Chloro-3'-nitroacetophenone

CAS 5465-65-6

Molecular FormulaC8H6ClNO3

Molecular Weight199.59

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Mass

MS-IW-0754          
4'-chloro-3'-nitroacetophenone
C8H6ClNO3           (Mass of molecular ion:    199)

   Source Temperature: 130 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      43.0      18.6
      50.0       1.1
      63.0       1.5
      74.0       2.6
      75.0       6.0
      89.0       1.7
     110.0       8.9
     111.0       2.0
     112.0       2.9
     118.0       1.8
     125.0       1.1
     126.0       2.9
     138.0      31.9
     139.0       2.5
     140.0      10.5
     154.0       1.1
     184.0     100.0
     185.0       8.2
     186.0      32.7
     187.0       2.7
     199.0      38.9
     200.0       3.6
     201.0      12.8
     202.0       1.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₆ Cl N O₃	0.036 g : 0.5 ml CDCl₃
4'-chloro-3'-nitroacetophenone

    Assign.     Shift(ppm)

      A             8.425
      B             8.102
      C             7.695
      D             2.667

     Hz     ppm     Int.

   3368.16   8.428    157
   3366.09   8.423    163
   3243.41   8.116    102
   3241.33   8.111     98
   3235.11   8.095    115
   3233.03   8.090    111
   3079.35   7.706    175
   3070.92   7.685    160
   1065.80   2.667   1000

in CDCl3