[1,1-Biphenyl]-2,5-diol,4-chloro-(9CI) synthesis
- Product Name:[1,1-Biphenyl]-2,5-diol,4-chloro-(9CI)
- CAS Number:10551-37-8
- Molecular formula:C12H9ClO2
- Molecular Weight:220.65
Yield:10551-37-8 79%
Reaction Conditions:
Stage #1: p-chlorobenzenediazonium tetrafluoroborate;hydroquinonewith hydrogenchloride;titanium(III) chloride in water;acetonitrile; for 0.583333 h;
Stage #2: with sodium hydroxide;sodium sulfite in water;
References:
Wetzel, Alexander;Ehrhardt, Varinia;Heinrich, Markus R. [Angewandte Chemie - International Edition,2008,vol. 47,# 47,p. 9130 - 9133] Location in patent:supporting information; experimental part
20307-43-1
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