2-(4-Chlorophenyl)cyclohexa-2,5-diene-1,4-dione synthesis
- Product Name:2-(4-Chlorophenyl)cyclohexa-2,5-diene-1,4-dione
- CAS Number:20307-43-1
- Molecular formula:C12H7ClO2
- Molecular Weight:218.64
Yield:20307-43-1 87%
Reaction Conditions:
Stage #1: 4-chloro-anilinewith tert.-butylnitrite;methyl bisulfate in water at 25; for 0.0833333 h;
Stage #2: p-benzoquinone in water at 40; for 24 h;Meerwein Arylation;Reagent/catalyst;
References:
Honraedt, Aurelien;Le Callonnec, Francois;Le Grognec, Erwan;Fernandez, Vincent;Felpin, Francois-Xavier [Journal of Organic Chemistry,2013,vol. 78,# 9,p. 4604 - 4609]
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106-51-4
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20307-43-1
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