1,1'-Oxydi-2-propanol synthesis
- Product Name:1,1'-Oxydi-2-propanol
- CAS Number:110-98-5
- Molecular formula:C6H14O3
- Molecular Weight:134.17
57-55-6
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110-98-5
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Yield:110-98-5 13 %Chromat.
Reaction Conditions:
with amberlyst 36Dry at 130;
Steps:
2.3. Catalyst testing
General procedure: The dehydration reaction was carried out in 5 mL glass vials which contained 5 g of propylene glycol, catalyst (0.25 g of zeolite or 0.043 g of Amberlyst 36Dry), and a stir bar. These vials were sealed with septa and placed in a circular multi-well aluminum heating block. Silicon oil was also used to improve contact between the well and the reactor vials. Temperature was monitored via a thermometer inserted into an identical vial containing propylene glycol and a stir bar. The reaction was carried out at 130 ?C unless otherwise specified. Vials were removed from the oil bath and quenched with ice-water to condense gas-phase products within the vial, and samples were drawn through the septum with a syringe.
References:
Courtney, Timothy D.;Nikolakis, Vladimiros;Mpourmpakis, Giannis;Chen, Jingguang G.;Vlachos, Dionisios G. [Applied Catalysis A: General,2012,vol. 449,p. 59 - 68]
