1,2,3,6-Tetrahydrophthalic anhydride synthesis
- Product Name:1,2,3,6-Tetrahydrophthalic anhydride
- CAS Number:85-43-8
- Molecular formula:C8H8O3
- Molecular Weight:152.15
108-31-6
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$13.47/50g
106-99-0
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$80.00/100mL
85-43-8
206 suppliers
$145.00/10g
Yield:85-43-8 98.1%
Reaction Conditions:
at 80 - 110; for 4 h;Large scale;Temperature;
Steps:
1-4 example 2
Maleic anhydride (490 g, 5 mol) was placed in a bubbling reactor, heated to 80 ° C to melt maleic anhydride, and continuously passed from the bottom of the bubbling reactor1,3-butadiene gas,The reaction temperature was controlled to 110 ° C. After 4 hours of reaction, the gas phase was detected, the reaction of the starting material was completed, and the temperature was solidified to obtain 746.3 g of a white solid. The yield was 98.1%.
References:
CN108586398,2018,A Location in patent:Page/Page column 4-6
95-47-6
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85-43-8
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$145.00/10g
88-98-2
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85-43-8
206 suppliers
$145.00/10g
108-31-6
873 suppliers
$13.47/50g
590-19-2
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$225.00/5G
85-43-8
206 suppliers
$145.00/10g