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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 1,5-DIHYDROXY-PENTAN-3-ONE
4254-85-7

1,5-DIHYDROXY-PENTAN-3-ONE synthesis

4synthesis methods
105-50-0 Synthesis
Diethyl 1,3-acetonedicarboxylate

105-50-0
407 suppliers
$6.00/5g

1,5-DIHYDROXY-PENTAN-3-ONE

4254-85-7
48 suppliers
$45.00/10mg

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / toluene / 12 h / Reflux; Dean-Stark
2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere; Cooling with ice
3: toluene-4-sulfonic acid / acetone / 1.5 h / 20 °C

References:

Pan, Sijun;Jang, Se-Young;Wang, Danyang;Liew, Si Si;Li, Zhengqiu;Lee, Jun-Seok;Yao, Shao Q. [Angewandte Chemie - International Edition,2017,vol. 56,# 39,p. 11816 - 11821][Angew. Chem.,2017,vol. 129,# 39,p. 11978 - 11983,6]

1,3-DIOXOLANE-2,2-DIETHANOL

5694-95-1
73 suppliers
$45.00/25mg

1,5-DIHYDROXY-PENTAN-3-ONE

4254-85-7
48 suppliers
$45.00/10mg

References
1,3-DIOXOLANE-2,2-DIACETIC ACID DIETHYL ESTER

71022-90-7
20 suppliers
$251.00/1g

1,5-DIHYDROXY-PENTAN-3-ONE

4254-85-7
48 suppliers
$45.00/10mg

References
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
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1,5-DIHYDROXY-PENTAN-3-ONE

4254-85-7
48 suppliers
$45.00/10mg

References

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